Simultaneous determination of fumonisins B1 and B2 in different types of maize by matrix solid phase dispersion and HPLC-MS/MS
نویسندگان
چکیده
منابع مشابه
Determination of Malathion and α-Endosulfan Residue in Khazar Rice Using Matrix Solid Phase Dispersion and HPLC
An extraction method based on matrix solid phase dispersion (MSPD) and high performance liquid chromatography with UV detection for quantification of two widely used pesticides (Malathion and α-Endosulfan) in Khazar rice from north of Iran were investigated. The ratio of solid phase (adsorbent) to sample, types of eluting solvent and its volume were optimized to achieve the highest recoveries f...
متن کامل[Determination of benzo[a]pyrene in vegetable oils by HPLC coupled with matrix solid phase dispersion].
Determination of benzo(a)pyrene in vegetable oils was carried out using aluminium oxide for clean-up followed by reverse phase high performance liquid chromatographic (HPLC). A quantity of oil was dissolved in petroleum ether and added to an aluminium oxide column which retained the lipids. Benzo(a)pyrene in the oil was eluted from the column with petroleum ether and the collected eluate was co...
متن کاملdetermination of malathion and α-endosulfan residue in khazar rice using matrix solid phase dispersion and hplc
an extraction method based on matrix solid phase dispersion (mspd) and high performance liquid chromatography with uv detection for quantification of two widely used pesticides (malathion and α-endosulfan) in khazar rice from north of iran were investigated. the ratio of solid phase (adsorbent) to sample, types of eluting solvent and its volume were optimized to achieve the highest recoveries f...
متن کاملdetermination of olanzapine and thiourea using electrodes modified by dna and film of copper-cobalt hexacyanoferrate & investigation of electro-oxidation of some catechol derivatives in the presence of 4-phenylsemicarbazid
چکیده هدف از این کار بررسی الکترواکسیداسیون کتکول و مشتقات آن در حضور 4-فنیل سمی کاربامازید بوده است اکسیداسیون کتکولها ترکیبات نا پایدار کینونها را تولید می کنند که این ترکیبات می تواند در واکنش مایکل بعنوان پذیرنده نوکلئوفیل عمل نمایند. در ادامه اکسایش کتکولهای (a-c1) را درحضور 4-فنیل سمی کاربامازید در محلول آب/استونیتریل (90/10)بوسیله ولتامتری چرخه ای و کولن متری در پتانسیل ثابت مورد بررسی ...
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ژورنال
عنوان ژورنال: Food Chemistry
سال: 2017
ISSN: 0308-8146
DOI: 10.1016/j.foodchem.2017.04.091